Gas Chromatography Detector: An Overview
by Emily John Digital Marketing Service ProviderThe detector senses the
presence of the individual components as they leave the column. The doctor out
pout after amplification is traced on a recorder. The duration of the intervals
is usually a single second or even less than that. Hence, the gas chromatography
detector is considered to be the brain of the instrument. The detector converts
a change in effluent into an electric signal that is recorded by the data
system.
Ideal
Properties of a detector
This gas
chromatography detector is used in both GC and HPLC should have the
following ideal properties:
·
High Sensitivity.
·
Good stability and reproducibility.
·
A linear response to solutes.
·
Negligible baseline noise.
·
It should be inexpensive.
·
Capable of providing information on the identity
of the solute.
·
A temperature range from room temperature to at
rest 400°C
·
The response is short for time independent of the
flow rate.
·
High reliability and ease of operation.
·
The detector should be non-destructive.
·
Response is independent of
mobile phase composition.
Detectors
used in GC
Detection devices for a GC must
respond rapidly and reproducibility to the low concentrations of the solutes
emitted from the column.
Concentration-dependent
detectors:
1.
Thermal conductivity detector
2.
Electron capture detector
3.
Argon ionization detector
4.
Helium ionization detector
Mass flow-dependent detectors:
1.
Flame ionization detector
2.
Nitrogen phosphorous detector
3. Flame photometric detector.
·
These
other detectors also used:
1.
Thermionic detectors
2.
Photoionization detectors
3.
Atomic emission detectors
4. Sulfur chemiluminescence detector
·
The
most widely used detectors are TCD, FID, and ECD.
TCD is known as a thermal
conductivity detector, which is one of the old detectors for GC, is still
widely in use. It is well known as a cathetometer and a hot wire detector. The
principle in TCD is the change in the thermal conductivity of the gas stream.
It is a simple, inexpensive, accurate, and non-destructive type.
FID is another most widely used
and generally applicable detector for GC. Detection involves monitoring the
current produced by collecting this charge carries. There are numbers of
properties performed by FID which makes the most useful general detector.
The electro-capture detector
used for environmental samples because it selectively responds to halogen-containing
organic compounds.
The final take
The detector is the key element that is present in any device that is used for the identification and estimation of any compound. It detects at a faster rate i.e. within seconds hence it is considered as brain if the instrument. Without a gas chromatography detector, no one can analyze the compound. Hence, it attains such important in the field of analysis.
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Created on Aug 9th 2019 06:05. Viewed 267 times.